(S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

Base Information

• Chemical Name: (S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide
• CAS No.: 1446512-90-8
• Molecular Formula: C₂₃H₂₅N₃O₉S
• Molecular Weight: 519.532

Synonyms:(S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

Chemical Property of (S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

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Technology Process of (S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

There total 1 articles about (S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester (4326-36-7) + 3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (66074-00-8) → (S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (1446512-90-8)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1039/c3ob41047a

Reference yield: 100.0%

(S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (1446512-90-8) → (S)-4-(4-(2-amino-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole-2-oxide hydrochloride (1446512-96-4)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; water;

DOI:10.1039/c3ob41047a

Reference yield: 90.0%

(S)-4-(4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (1446512-90-8) → (S)-4-(4-(2-((tert-butoxycarbonyl)amino)-2-carboxyethyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (1446512-97-5)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/c3ob41047a

upstream raw materials:

(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

Downstream raw materials:

(S)-4-(4-(2-amino-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole-2-oxide hydrochloride

(S)-4-(4-(2-((tert-butoxycarbonyl)amino)-2-carboxyethyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

(S)-4-(4-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole2-oxide

(S)-4-(4-(2-((allyloxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)-3-(phenylsulfonyl)-1,2,5-oxadiazole-2-oxide

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