2-iodo-6-methoxy-N-methyl-N-tosylaniline

Base Information

Chemical Name:2-iodo-6-methoxy-N-methyl-N-tosylaniline
CAS No.:937390-82-4
Molecular Formula:C₁₅H₁₆INO₃S
Molecular Weight:417.267
Hs Code.:

Synonyms:2-iodo-6-methoxy-N-methyl-N-tosylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-iodo-6-methoxy-N-methyl-N-tosylaniline

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Technology Process of 2-iodo-6-methoxy-N-methyl-N-tosylaniline

There total 6 articles about 2-iodo-6-methoxy-N-methyl-N-tosylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 937390-81-3
2-iodo-6-methoxy-N-tosylaniline

: 74-88-4
methyl iodide

: 937390-82-4
2-iodo-6-methoxy-N-methyl-N-tosylaniline

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1002/anie.200604038

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 937390-82-4
2-iodo-6-methoxy-N-methyl-N-tosylaniline

Guidance literature:: Multi-step reaction with 5 steps

1.1: 100 percent / tetrahydrofuran / Heating

2.1: t-BuLi / diethyl ether; pentane / 3 h / -20 °C

2.2: 47 percent / iodine / diethyl ether; pentane / -90 - 20 °C

3.1: CF₃COOH / CH₂Cl₂ / 3 h / 20 °C

4.1: 2.27 g / pyridine / 20 °C

5.1: 96 percent / NaH / dimethylformamide; various solvent(s) / 5 h / 20 °C

With pyridine; tert.-butyl lithium; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; pentane;
DOI:10.1002/anie.200604038

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 937390-82-4
2-iodo-6-methoxy-N-methyl-N-tosylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 2.27 g / pyridine / 20 °C

2: 96 percent / NaH / dimethylformamide; various solvent(s) / 5 h / 20 °C

With pyridine; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200604038