1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ³-benzo[d][1,2]iodoxole

Base Information

• Chemical Name: 1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ³-benzo[d][1,2]iodoxole
• CAS No.: 182884-09-9
• Molecular Formula: C₁₄H₁₂ClIO
• Molecular Weight: 358.606
• Mol file: 182884-09-9.mol

Synonyms:1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ³-benzo[d][1,2]iodoxole

Chemical Property of 1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ³-benzo[d][1,2]iodoxole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ³-benzo[d][1,2]iodoxole

There total 1 articles about 1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ³-benzo[d][1,2]iodoxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-(2-iodophenyl)-1-phenylethan-1-ol (182884-20-4) → 1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ3-benzo[d][1,2]iodoxole (182884-09-9)

Guidance literature:

With tert-butylhypochlorite; In dichloromethane;

DOI:10.1016/j.tet.2010.04.125

Reference yield: 83.0%

1-Chloro-3-methyl-3-phenyl-1,3-dihydro-1λ3-benzo[d][1,2]iodoxole (182884-09-9) → 1-azido-1,3-dihydro-3-methyl-3-phenyl-1,2-benziodoxole

Guidance literature:

With sodium azide; In acetonitrile; for 2h; Ambient temperature;

DOI:10.1016/0040-4039(96)01436-0

upstream raw materials:

1-(2-iodophenyl)-1-phenylethan-1-ol