Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

Base Information

Chemical Name:Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester
CAS No.:131729-76-5
Molecular Formula:C₁₂H₁₄O₆
Molecular Weight:254.24
Hs Code.:

Synonyms:Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

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Chemical Property of Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

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Technology Process of Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

There total 3 articles about Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 133415-58-4
<2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

: 131729-76-5
Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; for 18h; under 4137.2 Torr;
DOI:10.1021/jm00105a058

Reference yield:

: 100899-56-7
2,2-Dimethyl-4-phenoxycarbonyloxymethyl-1,3-dioxolane

: 131729-76-5
Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: camphorsulfonic acid (CSA) / toluene / 18 h / Ambient temperature

2: 93 percent / H₂ / 5percent Pd/C / CH₂Cl₂; ethanol / 18 h / 4137.2 Torr

With camphor-10-sulfonic acid; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; toluene;
DOI:10.1021/jm00105a058

Reference yield:

: 1885-14-9
phenyl chloroformate

: 131729-76-5
Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

2: camphorsulfonic acid (CSA) / toluene / 18 h / Ambient temperature

3: 93 percent / H₂ / 5percent Pd/C / CH₂Cl₂; ethanol / 18 h / 4137.2 Torr

With pyridine; camphor-10-sulfonic acid; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; toluene;
DOI:10.1021/jm00105a058