Technology Process of C23H32O2Si
There total 6 articles about C23H32O2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
vinylbenzyl bromide;
With
magnesium; ethylene dibromide;
In
diethyl ether;
at 20 ℃;
for 2h;
Inert atmosphere;
1-(2-(((1,1-dimethylethyl)dimethylsilyl)oxy)phenyl)ethanone;
In
diethyl ether;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1039/c1ob05725a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
2.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
2.2: 0.42 h / 0 °C / Inert atmosphere
3.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere
3.2: 1 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; magnesium; ethylene dibromide; triphenylphosphine;
In
diethyl ether; dichloromethane;
DOI:10.1039/c1ob05725a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
3.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
3.2: 0.42 h / 0 °C / Inert atmosphere
4.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere
4.2: 1 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; potassium tert-butylate; magnesium; ethylene dibromide; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; dichloromethane;
1.1: Wittig olefination;
DOI:10.1039/c1ob05725a
