Technology Process of C23H32O2Si
There total 6 articles about C23H32O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
vinylbenzyl bromide;
With
magnesium; ethylene dibromide;
In
diethyl ether;
at 20 ℃;
for 2h;
Inert atmosphere;
1-(2-(((1,1-dimethylethyl)dimethylsilyl)oxy)phenyl)ethanone;
In
diethyl ether;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1039/c1ob05725a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
2.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
2.2: 0.42 h / 0 °C / Inert atmosphere
3.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere
3.2: 1 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; magnesium; ethylene dibromide; triphenylphosphine;
In
diethyl ether; dichloromethane;
DOI:10.1039/c1ob05725a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
3.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
3.2: 0.42 h / 0 °C / Inert atmosphere
4.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere
4.2: 1 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; potassium tert-butylate; magnesium; ethylene dibromide; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; dichloromethane;
1.1: Wittig olefination;
DOI:10.1039/c1ob05725a