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C23H32O2Si

Base Information Edit
C<sub>23</sub>H<sub>32</sub>O<sub>2</sub>Si

Synonyms:C23H32O2Si

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Chemical Property of C23H32O2Si Edit
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Technology Process of C23H32O2Si

There total 6 articles about C23H32O2Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
vinylbenzyl bromide; With magnesium; ethylene dibromide; In diethyl ether; at 20 ℃; for 2h; Inert atmosphere;
1-(2-(((1,1-dimethylethyl)dimethylsilyl)oxy)phenyl)ethanone; In diethyl ether; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c1ob05725a
Guidance literature:
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
2.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
2.2: 0.42 h / 0 °C / Inert atmosphere
3.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere
3.2: 1 h / 20 °C / Inert atmosphere
With lithium aluminium tetrahydride; magnesium; ethylene dibromide; triphenylphosphine; In diethyl ether; dichloromethane;
DOI:10.1039/c1ob05725a
Guidance literature:
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
3.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
3.2: 0.42 h / 0 °C / Inert atmosphere
4.1: magnesium; ethylene dibromide / diethyl ether / 2 h / 20 °C / Inert atmosphere
4.2: 1 h / 20 °C / Inert atmosphere
With lithium aluminium tetrahydride; potassium tert-butylate; magnesium; ethylene dibromide; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Wittig olefination;
DOI:10.1039/c1ob05725a
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