tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane

Base Information

Chemical Name:tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane
CAS No.:943529-63-3
Molecular Formula:C₂₂H₄₀O₃Si
Molecular Weight:380.643
Hs Code.:

Synonyms:tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane

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Chemical Property of tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane

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Technology Process of tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane

There total 2 articles about tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 943529-62-2
(3R)-1-[(4-methoxybenzyl)oxy]octan-3-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 943529-63-3
tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1080/00397910701229107

Reference yield:

: 195257-60-4
(2S)-2-[2-(p-methoxybenzyloxy)ethyl]oxirane

: 943529-63-3
tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(I) iodide / diethyl ether; hexane / 0.5 h / -20 °C

1.2: 87 percent / diethyl ether / 1 h / -20 °C

2.1: 74 percent / imidazole / CH₂Cl₂ / 2 h / 0 °C

With 1H-imidazole; copper(l) iodide; In diethyl ether; hexane; dichloromethane;
DOI:10.1080/00397910701229107

Reference yield:

: 943529-63-3
tert-butyl[((1R)-1-{2-[(4-methoxybenzyl)oxy]ethyl}hexyl)oxy]dimethylsilane

: 51154-96-2,54814-64-1
(R)-massoialactone

Guidance literature:: Multi-step reaction with 4 steps

1.1: 80 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; H₂O / CH₂Cl₂ / 3 h / 20 °C

2.1: 68 percent / 2-iodoxybenzoic acid / dimethylsulfoxide; CH₂Cl₂ / 2 h / 20 °C

3.1: NaH / tetrahydrofuran / 0 °C

3.2: 85 percent / tetrahydrofuran / 2 h

4.1: p-TsOH / methanol / 0.5 h / 20 °C

4.2: 76 percent / benzene / 1 h / 20 °C

With water; sodium hydride; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; 3.2: Horner-Wadsworth-Emmons reaction;
DOI:10.1080/00397910701229107