C₃₁H₃₄O₈S

Base Information

Chemical Name:C₃₁H₃₄O₈S
CAS No.:1432045-89-0
Molecular Formula:C₃₁H₃₄O₈S
Molecular Weight:566.672
Hs Code.:

C<sub>31</sub>H<sub>34</sub>O<sub>8</sub>S

Synonyms:C₃₁H₃₄O₈S

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Chemical Property of C₃₁H₃₄O₈S

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Technology Process of C₃₁H₃₄O₈S

There total 8 articles about C₃₁H₃₄O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1432045-88-9
C₃₁H₃₅IO₈S

: 1432045-89-0
C₃₁H₃₄O₈S

Guidance literature:: With 1,1'-[(1S)-(1,1'-binaphthalene)-2,2'-diyl]bis[1,1-di-tert-butyl-phosphine]; palladium diacetate; caesium carbonate; In toluene; at 50 ℃; for 12h;
DOI:10.1016/j.bmcl.2013.03.060

Reference yield:

: 1000413-84-2
2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-carbaldehyde

: 1432045-89-0
C₃₁H₃₄O₈S

Guidance literature:: Multi-step reaction with 6 steps

1: 1,4-dioxane; water / 12 h / 100 °C

2: AD-mix-α / water; tert-butyl alcohol / 4 h / 0 - 20 °C

3: 1H-imidazole; dmap / N,N-dimethyl-formamide / 1 h / 20 °C

4: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 1 h / 50 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

6: palladium diacetate; 1,1'-[(1S)-(1,1'-binaphthalene)-2,2'-diyl]bis[1,1-di-tert-butyl-phosphine]; caesium carbonate / toluene / 12 h / 50 °C

With 1H-imidazole; dmap; tributylphosphine; AD-mix-α; 1,1'-[(1S)-(1,1'-binaphthalene)-2,2'-diyl]bis[1,1-di-tert-butyl-phosphine]; tetrabutyl ammonium fluoride; palladium diacetate; caesium carbonate; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1: |Wittig Olefination / 2: |Sharpless Dihydroxylation / 4: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2013.03.060

Reference yield:

: 1430232-70-4
(S)-2-(6-hydroxy-5-iodo-2,3-dihydrobenzofuran-3-yl)acetic acid methyl ester

: 1432045-89-0
C₃₁H₃₄O₈S

Guidance literature:: Multi-step reaction with 3 steps

1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 1 h / 50 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

3: palladium diacetate; 1,1'-[(1S)-(1,1'-binaphthalene)-2,2'-diyl]bis[1,1-di-tert-butyl-phosphine]; caesium carbonate / toluene / 12 h / 50 °C

With tributylphosphine; 1,1'-[(1S)-(1,1'-binaphthalene)-2,2'-diyl]bis[1,1-di-tert-butyl-phosphine]; tetrabutyl ammonium fluoride; palladium diacetate; caesium carbonate; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; toluene; 1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2013.03.060