2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine

Base Information

Chemical Name:2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine
CAS No.:1610450-59-3
Molecular Formula:C₁₅H₂₄N₂O₆
Molecular Weight:328.365
Hs Code.:

Synonyms:2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine

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Chemical Property of 2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine

Chemical Property:

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Technology Process of 2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine

There total 2 articles about 2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2741-30-2
1-O<2'-Dimethylaminoethoxyethyl>ethylenglykol

: 7145-49-5
3-methoxy-5-nitrophenol

: 1610450-59-3
2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 18h;

Reference yield:

: 16618-67-0
3-bromo-5-nitroanisole

: 1610450-59-3
2-(2-(2-(3-methoxy-5-nitrophenoxy)ethoxy)ethoxy)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium hydroxide; tert-butyl XPhos / 1,4-dioxane; water / 2 h / 100 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 18 h / 0 - 20 °C

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; di-isopropyl azodicarboxylate; triphenylphosphine; potassium hydroxide; tert-butyl XPhos; In tetrahydrofuran; 1,4-dioxane; water;