[(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester

Base Information

• Chemical Name: [(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester
• CAS No.: 64370-13-4
• Molecular Formula: C₂₇H₂₀N₄O₈S₃
• Molecular Weight: 624.676

Synonyms:[(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester

Chemical Property of [(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester

Chemical Property:

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Technology Process of [(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester

There total 2 articles about [(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrobenzyl (2R,3R)-2-(benzothiazol-2'-yldithio)-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine-1-acetate (64370-08-7) → [(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester (64370-13-4)

Guidance literature:

With ozone; In acetic acid methyl ester; at -78 ℃;

DOI:10.1021/ja00494a032

Reference yield:

→ [(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester (64370-13-4)

Guidance literature:

entspr. Propylidenverb. , Ozon;

Reference yield:

[(2R)-2r-benzothiazol-2-yldisulfanyl-4-oxo-3c-(2-phenoxy-acetylamino)-azetidin-1-yl]-oxo-acetic acid 4-nitro-benzyl ester (64370-13-4) → (3R,4R)-4-(benzothiazol-2-yl)dithio-3-phenoxyacetamido-2-oxoazetidine (64370-14-5)

Guidance literature:

In methanol; acetic acid methyl ester; water; for 0.333333h; Heating;

DOI:10.1021/ja00494a032

upstream raw materials:

p-nitrobenzyl (2R,3R)-2-(benzothiazol-2'-yldithio)-α-isopropylidene-4-oxo-3-phenoxyacetylaminoazetidine-1-acetate

Downstream raw materials:

(3R,4R)-4-(benzothiazol-2-yl)dithio-3-phenoxyacetamido-2-oxoazetidine

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