(4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

Base Information

Chemical Name:(4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine
CAS No.:77232-47-4
Molecular Formula:C₂₄H₁₈ClN₃O
Molecular Weight:399.879
Hs Code.:

Synonyms:(4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

Suppliers and Price of (4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

There total 5 articles about (4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1670-14-0
benzamidine monohydrochloride

: 77232-47-4
(4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 6 steps

1: 65.8 percent / sodium methylate / ethanol / 4 h / Heating

2: 90.2 percent / phosphorus oxychloride, triethylamine / 10 - 100 deg C during 1 h, 100 - 105 deg C 1 h

3: 96.7 percent / methanol / 5 h / Heating

4: 74.9 percent / N-bromosuccinimide, dibenzoylperoxide, α,α'-azoisobutyronitrile / CCl4 / 3 h / Heating; Irradiation

5: 58.1 percent / sodium, ethanol, 2-nitropropane / dimethylformamide / 2 h / 60 - 65 °C

6: 69.3 percent / boric acid / xylene / 3 h / Heating

With N-Bromosuccinimide; ethanol; 2-nitropropane; azobisisobutyronitrile; sodium methylate; boric acid; sodium; triethylamine; trichlorophosphate; dibenzoyl peroxide; In methanol; tetrachloromethane; ethanol; N,N-dimethyl-formamide; xylene;
DOI:10.1002/hlca.19810640114

Reference yield:

: 77232-16-7
6-Chlor-2-phenyl-4-(p-tolyl)pyrimidin

: 77232-47-4
(4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 96.7 percent / methanol / 5 h / Heating

2: 74.9 percent / N-bromosuccinimide, dibenzoylperoxide, α,α'-azoisobutyronitrile / CCl4 / 3 h / Heating; Irradiation

3: 58.1 percent / sodium, ethanol, 2-nitropropane / dimethylformamide / 2 h / 60 - 65 °C

4: 69.3 percent / boric acid / xylene / 3 h / Heating

With N-Bromosuccinimide; ethanol; 2-nitropropane; azobisisobutyronitrile; boric acid; sodium; dibenzoyl peroxide; In methanol; tetrachloromethane; N,N-dimethyl-formamide; xylene;
DOI:10.1002/hlca.19810640114

Reference yield:

: 77232-15-6
6-Hydroxy-2-phenyl-4-(p-tolyl)pyrimidin

: 77232-47-4
(4-Chloro-phenyl)-[1-[4-(6-methoxy-2-phenyl-pyrimidin-4-yl)-phenyl]-meth-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 90.2 percent / phosphorus oxychloride, triethylamine / 10 - 100 deg C during 1 h, 100 - 105 deg C 1 h

2: 96.7 percent / methanol / 5 h / Heating

3: 74.9 percent / N-bromosuccinimide, dibenzoylperoxide, α,α'-azoisobutyronitrile / CCl4 / 3 h / Heating; Irradiation

4: 58.1 percent / sodium, ethanol, 2-nitropropane / dimethylformamide / 2 h / 60 - 65 °C

5: 69.3 percent / boric acid / xylene / 3 h / Heating

With N-Bromosuccinimide; ethanol; 2-nitropropane; azobisisobutyronitrile; boric acid; sodium; triethylamine; trichlorophosphate; dibenzoyl peroxide; In methanol; tetrachloromethane; N,N-dimethyl-formamide; xylene;
DOI:10.1002/hlca.19810640114