Technology Process of C13H21N3O4
There total 1 articles about C13H21N3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / Heating
2: pyridinium chlorochromate / dichloromethane / 20 °C
3: sulfuric acid / dichloromethane; acetonitrile / 1 h
4: lithium aluminium tetrahydride / diethyl ether
5: methanesulfonyl chloride; pyridine
With
pyridine; lithium aluminium tetrahydride; sulfuric acid; potassium carbonate; methanesulfonyl chloride; pyridinium chlorochromate;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.2298/JSC150430063O
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / diethyl ether
2: dichloromethane / 0.75 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride;
In
diethyl ether; dichloromethane;
DOI:10.2298/JSC150430063O
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / diethyl ether
2: dichloromethane / 2 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride;
In
diethyl ether; dichloromethane;
DOI:10.2298/JSC150430063O