methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Base Information

Chemical Name:methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate
CAS No.:1610860-40-6
Molecular Formula:C₁₇H₂₇N₃O₅S
Molecular Weight:385.484
Hs Code.:

Synonyms:methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

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Chemical Property of methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Chemical Property:

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Technology Process of methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

There total 5 articles about methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 109-01-3
1-methyl-piperazine

: 1610860-39-3
methyl 3-(N-(2-bromoethyl)methylsulfonamido)-4-methoxybenzoate

: 1610860-40-6
methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 130 ℃; for 3h; Microwave irradiation;

Reference yield:

: 2840-26-8
3-amino-4-methoxybenzoic acid

: 1610860-40-6
methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 24 h / Reflux

2: pyridine / 3 h / 0 - 20 °C

3: potassium carbonate / acetonitrile / 5 h / 110 °C / Microwave irradiation

4: triphenylphosphine; carbon tetrabromide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5: potassium carbonate / acetonitrile / 3 h / 130 °C / Microwave irradiation

With pyridine; carbon tetrabromide; sulfuric acid; potassium carbonate; triphenylphosphine; In dichloromethane; acetonitrile;

Reference yield:

: 29655-68-3
methyl 4-methoxy-3-(methylsulfonamido)benzoate

: 1610860-40-6
methyl 4-methoxy-3-(N-(2-(4-methylpiperazin-1-yl)ethyl)methylsulfonamido)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 5 h / 110 °C / Microwave irradiation

2: triphenylphosphine; carbon tetrabromide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3: potassium carbonate / acetonitrile / 3 h / 130 °C / Microwave irradiation

With carbon tetrabromide; potassium carbonate; triphenylphosphine; In dichloromethane; acetonitrile;