2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate

Base Information

Chemical Name:2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate
CAS No.:219674-28-9
Molecular Formula:C₂₀H₂₈N₂O₅
Molecular Weight:376.453
Hs Code.:

Synonyms:2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate

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Chemical Property of 2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate

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Technology Process of 2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate

There total 1 articles about 2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 25616-33-5
2-((2S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)acetic acid

: 513-42-8
3-hydroxy-2-methyl-1-propene

: 219674-28-9
2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -15 ℃;
DOI:10.1002/1099-0690(200004)2000:7<1241::AID-EJOC1241>3.0.CO;2-U

Reference yield:

: 219674-28-9
2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate

: (R)-2-((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pent-4-enoic acid

: (S)-2-((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-4-methyl-pent-4-enoic acid

Guidance literature:: With manganese(ll) chloride; lithium diisopropyl amide; In tetrahydrofuran; at -78 - 20 ℃; Title compound not separated from byproducts;
DOI:10.1039/a805784b

Reference yield:

: 219674-28-9
2-methylallyl N-(tert-butyloxycarbonyl)-(S)-phenylalanylglycinate

: [N-(tert-butyloxycarbonyl)phenylalanyl]-4,5-didehydroleucine

Guidance literature:: With zinc(II) chloride; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1.) -78 deg C, 10 min; r.t., 16 h;
DOI:10.1021/jo00101a026