(S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate

Base Information

Chemical Name:(S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate
CAS No.:952152-72-6
Molecular Formula:C₂₂H₂₂F₂N₆O₄S
Molecular Weight:504.517
Hs Code.:

(S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate

Synonyms:(S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate

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Chemical Property of (S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate

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Technology Process of (S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate

There total 2 articles about (S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₁ClF₂N₆O₆S

: 952152-72-6
(S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/j.ejmech.2013.08.002

Reference yield:

: 49609-84-9
2-Chloronicotinoyl chloride

: 952151-87-0
O-methyl (S)-N-(3-(4-(1-(tert-butoxycarbonyl)[1,2,5]triazepan-5-yl)-3,5-difluorophenyl)-2-oxooxazolidin-5-yl)methylthiocarbamate

: 952152-72-6
(S)-N-((3-(3,5-difluoro-4-(10-oxo-5,6,8,9-tetrahydro-10H-4,4b,7,9a-tetraazabenzo[a]azulen-7-yl)phenyl)-2-oxo-5-oxazolidinyl)methyl)-O-methylthiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 18 h / 20 °C

With pyridine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.ejmech.2013.08.002