C₃₀H₂₈Cl₂O₆

Base Information

Chemical Name:C₃₀H₂₈Cl₂O₆
CAS No.:1616766-80-3
Molecular Formula:C₃₀H₂₈Cl₂O₆
Molecular Weight:555.455
Hs Code.:

C<sub>30</sub>H<sub>28</sub>Cl<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₀H₂₈Cl₂O₆

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Chemical Property of C₃₀H₂₈Cl₂O₆

Chemical Property:

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Technology Process of C₃₀H₂₈Cl₂O₆

There total 9 articles about C₃₀H₂₈Cl₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1616766-74-5
4-[(1Z,3E)-1-chloro-5-methylhexa-1,3,5-trien-1-yl]benzoic acid

: 1616766-75-6
(R)-4-[2-(4-chlorobenzoyloxy)ethyl]cyclohexa-1,5-diene-1-carboxylic acid

: 1616766-80-3
C₃₀H₂₈Cl₂O₆

Guidance literature:: With (2-bromophenyl)boronic acid; In 1,2-dichloro-ethane; for 18h; Reflux;
DOI:10.1039/c4cc01830c

Reference yield:

: 1616766-87-0
methyl 4-((triisopropylsilyl)ethynyl)benzoate

: 1616766-80-3
C₃₀H₂₈Cl₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide; silver fluoride / acetonitrile / 18 h / 20 °C / Darkness

2: lithium chloride; bis(η3-allyl-μ-chloropalladium(II)); 1,5-cis,cis-cyclooctadiene; acetic acid / 18 h / 80 °C

3: lithium hydroxide monohydrate / tetrahydrofuran; water / 6 h / 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / tetrahydrofuran; water / 6 h / 50 °C / Darkness

5: (2-bromophenyl)boronic acid / 1,2-dichloro-ethane / 18 h / Reflux

With potassium phosphate; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; bis(η3-allyl-μ-chloropalladium(II)); lithium hydroxide monohydrate; silver fluoride; acetic acid; lithium chloride; (2-bromophenyl)boronic acid; In tetrahydrofuran; water; 1,2-dichloro-ethane; acetonitrile; 5: |Diels-Alder Cycloaddition;
DOI:10.1039/c4cc01830c

Reference yield:

: 619-44-3
methyl 4-iodobenzoate

: 1616766-80-3
C₃₀H₂₈Cl₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 18 h / 20 °C / Inert atmosphere

2: N-Bromosuccinimide; silver fluoride / acetonitrile / 18 h / 20 °C / Darkness

3: lithium chloride; bis(η3-allyl-μ-chloropalladium(II)); 1,5-cis,cis-cyclooctadiene; acetic acid / 18 h / 80 °C

4: lithium hydroxide monohydrate / tetrahydrofuran; water / 6 h / 20 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate / tetrahydrofuran; water / 6 h / 50 °C / Darkness

6: (2-bromophenyl)boronic acid / 1,2-dichloro-ethane / 18 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; bis(η3-allyl-μ-chloropalladium(II)); lithium hydroxide monohydrate; silver fluoride; acetic acid; triethylamine; lithium chloride; (2-bromophenyl)boronic acid; In tetrahydrofuran; water; 1,2-dichloro-ethane; acetonitrile; 1: |Sonogashira Cross-Coupling / 6: |Diels-Alder Cycloaddition;
DOI:10.1039/c4cc01830c