(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime

Base Information

• Chemical Name: (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime
• CAS No.: 103869-96-1
• Molecular Formula: C₁₄H₁₆N₄O
• Molecular Weight: 256.307

Synonyms:(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime

Chemical Property of (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime

Chemical Property:

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Technology Process of (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime

There total 1 articles about (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one (97507-59-0) → (E)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime (103869-90-5) + (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime (103869-96-1)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; for 3h; Heating;

Reference yield: 87.0%

(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime (103869-96-1) + p-toluenesulfonyl chloride (98-59-9) → (Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate (128501-75-7)

Guidance literature:

With sodium hydroxide; In acetone; at 0 ℃; for 0.5h;

Reference yield: 5.0%

(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime (103869-96-1) → 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one (97507-59-0) + 5,6,7,8-tetrahydro-7,7-dimethyl-2-phenyl-1,2,3-triazol<4,5-c>azepin-4-one (128501-68-8)

Guidance literature:

With phosphorus pentachloride; In diethyl ether; for 2h; Ambient temperature;

upstream raw materials:

4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one

Downstream raw materials:

4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one

5,6,7,8-tetrahydro-7,7-dimethyl-2-phenyl-1,2,3-triazol<4,5-c>azepin-4-one

(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

4,6,7,8-tetrahydro-7,7-dimethyl-2-phenyl-5H-1,2,3-triazol<4,5-c>azepine

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