2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole

Base Information

Chemical Name:2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole
CAS No.:1350456-12-0
Molecular Formula:C₃₆H₂₃N₅
Molecular Weight:525.612
Hs Code.:

Synonyms:2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole

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Chemical Property of 2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole

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Technology Process of 2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole

There total 1 articles about 2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 138253-30-2
4'-(4-formylphenyl)-[2,2':6',2'']terpyridine

: 84-11-7
9,10-phenanthrenequinone

: 1350456-12-0
2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole

Guidance literature:: With ammonium acetate; In acetic acid; for 2h; Reflux;
DOI:10.1021/ic201610w

Reference yield: 70.0%

: 136276-24-9
[trichloro(4'-tolyl-2,2':6',2''-terpyridine)ruthenium(III)]

: 1350456-12-0
2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole

: sodium perchlorate

: 7732-18-5
water

: 67-64-1
acetone

: [(4'-(4-methylphenyl)-2,2':6',2''-terpyridine)Ru(2-(4-[2,2':6',2'']terpyridine-4'-yl-phenyl)-1H-phenanthro[9,10-d]-imidazole)](ClO₄)2*2H₂O

Guidance literature:: With AgBF₄; In ethanol; byproducts: AgCl; (N2); a mixt. of Ru complex, AgBF4 and acetone refluxed for 4 h, cooled to room temp., filtered, EtOH added, concd. (vac.), ligand added, refluxed for 12 h; cooled to room temp., filtered, washed (CHCl3 and ether), dried (vac.), dissolved in MeCN, chromd. (silica gel, MeCN), concd., anion-exchanged with NaClO4, recrystd. (MeCN/MeOH/aq. HClO4); elem. anal.;
DOI:10.1021/ic201610w