-p-iodobenzene

Base Information

• Chemical Name: -p-iodobenzene
• CAS No.: 73178-09-3
• Molecular Formula: C₁₃H₁₂I₂O₄S
• Molecular Weight: 518.111
• Mol file: 73178-09-3.mol

Synonyms:-p-iodobenzene

Chemical Property of -p-iodobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of -p-iodobenzene

There total 2 articles about -p-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

para-diiodobenzene (624-38-4,1032416-46-8) + -o-toluene (73177-97-6) → -p-iodobenzene (73178-09-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 168h; Darkness;

DOI:10.1016/j.tet.2012.03.113

Reference yield: 62.0%

para-diiodobenzene (624-38-4,1032416-46-8) + [hydroxy(tosyloxy)iodo]benzene (27126-76-7) → -p-iodobenzene (73178-09-3)

Guidance literature:

DOI:10.1021/jo01296a049

Reference yield: 85.0%

iodobenzene (591-50-4) + trifluorormethanesulfonic acid (1493-13-6) + -p-iodobenzene (73178-09-3) → 4,4'-diiododiphenyliodonium triflate

Guidance literature:

In dichloromethane; at -78 - 20 ℃; Darkness;

DOI:10.1016/j.tet.2012.03.113

upstream raw materials:

para-diiodobenzene

[hydroxy(tosyloxy)iodo]benzene

-o-toluene

Downstream raw materials:

(p-iodophenyl)(5-methyl-2-thienyl)iodonium tosylate

para-diiodobenzene

p-iodophenyl(2-furyl)iodonium tosylate

Toluene-4-sulfonate(4-iodo-phenyl)-(5-trimethylsilanyl-furan-2-yl)-iodonium;