4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde

Base Information

Chemical Name:4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde
CAS No.:1609537-11-2
Molecular Formula:C₁₆H₁₀ClFN₂O₂S
Molecular Weight:348.785
Hs Code.:

Synonyms:4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde

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Chemical Property of 4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde

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Technology Process of 4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde

There total 3 articles about 4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609536-79-9
(4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}phenyl)methanol

: 1609537-11-2
4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde

Guidance literature:: With periodic acid; pyridinium chlorochromate; In acetonitrile; at 0 - 20 ℃; for 1h;

Reference yield:

: 58855-42-8
4-(hydroxymethyl)benzoic hydrazide

: 1609537-11-2
4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethanol / 16 h / Reflux

2: sodium hydroxide / water / 16 h / 20 °C

3: pyridinium chlorochromate; periodic acid / acetonitrile / 1 h / 0 - 20 °C

With periodic acid; triethylamine; pyridinium chlorochromate; sodium hydroxide; In ethanol; water; acetonitrile;

Reference yield:

: 1609536-71-1
[4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl]methanol

: 1609537-11-2
4-{5-[(3-chloro-2-fluorobenzyl)thio]-1,3,4-oxadiazol-2-yl}benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 16 h / 20 °C

2: pyridinium chlorochromate; periodic acid / acetonitrile / 1 h / 0 - 20 °C

With periodic acid; pyridinium chlorochromate; sodium hydroxide; In water; acetonitrile;