C₃₆H₆₃ClO₇Si₂

Base Information

Chemical Name:C₃₆H₆₃ClO₇Si₂
CAS No.:916323-75-6
Molecular Formula:C₃₆H₆₃ClO₇Si₂
Molecular Weight:699.516
Hs Code.:

C<sub>36</sub>H<sub>63</sub>ClO<sub>7</sub>Si<sub>2</sub>

Synonyms:C₃₆H₆₃ClO₇Si₂

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Chemical Property of C₃₆H₆₃ClO₇Si₂

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Technology Process of C₃₆H₆₃ClO₇Si₂

There total 1 articles about C₃₆H₆₃ClO₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 916323-71-2
C₂₄H₃₃ClO₄

: 916323-75-6
C₃₆H₆₃ClO₇Si₂

Guidance literature:: DOI:10.1002/anie.200705565

Reference yield: 88.0%

: 916323-75-6
C₃₆H₆₃ClO₇Si₂

: 916323-63-2
C₃₀H₄₉ClO₇Si

Guidance literature:: With pyridinium p-toluenesulfonate; In methanol; dichloromethane; at 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1002/anie.201108594

Reference yield:

: 916323-75-6
C₃₆H₆₃ClO₇Si₂

: C₄₈H₈₇ClO₁₂Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogen / ethanol / 16 h / Inert atmosphere

2: 1H-imidazole / dichloromethane / 0.17 h / Inert atmosphere

3: pyridinium p-toluenesulfonate / methane; dichloromethane / 1.5 h / 0 °C / Inert atmosphere

4: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / Inert atmosphere

5: tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C / Inert atmosphere

6: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / Inert atmosphere

7: dimethyl sulfide borane / tetrahydrofuran / 2 h / Inert atmosphere

With 1H-imidazole; hydrogen; dimethyl sulfide borane; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; methane; ethanol; hexane; dichloromethane; 4: Dess-Martin oxidation / 5: Wittig olefination;
DOI:10.1039/c2ob25101a