3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ⁴δ²,5,2,4-trithiadiazepine

Base Information

• Chemical Name: 3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ⁴δ²,5,2,4-trithiadiazepine
• CAS No.: 131980-58-0
• Molecular Formula: C₁₅H₈Cl₂N₄S₃
• Molecular Weight: 411.359

Synonyms:3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ⁴δ²,5,2,4-trithiadiazepine

Chemical Property of 3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ⁴δ²,5,2,4-trithiadiazepine

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Technology Process of 3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ⁴δ²,5,2,4-trithiadiazepine

There total 1 articles about 3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ⁴δ²,5,2,4-trithiadiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

bis-(4-chlorophenyl)diazomethane (1143-92-6) + 6-bromo-1,3λ4δ2,5,2,4-trithiadiazepine (97484-11-2) → 3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ4δ2,5,2,4-trithiadiazepine (131980-58-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In methanol; for 0.333333h; Ambient temperature;

Reference yield: 27.0%

3,3-bis(4-chlorophenyl)-3H-pyrazolo<6,7-c>-1,3λ4δ2,5,2,4-trithiadiazepine (131980-58-0) → 8-(4-chlorophenyl)-5-chloroindeno<1,2-d>-1,2,3-dithiazole (131980-63-7)

Guidance literature:

at 210 ℃; for 0.00138889h;

DOI:10.1039/c39900001319

upstream raw materials:

bis-(4-chlorophenyl)diazomethane

6-bromo-1,3λ⁴δ²,5,2,4-trithiadiazepine

Downstream raw materials:

8-(4-chlorophenyl)-5-chloroindeno<1,2-d>-1,2,3-dithiazole

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