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Technology Process of IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4

IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4

Base Information
  • Chemical Name:IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4
  • CAS No.:190650-44-3
  • Molecular Formula:C24H39IrOP*C32H12BF24
  • Molecular Weight:1429.99
  • Hs Code.:
IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3<sup>(1+)</sup>*B((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4<sup>(1-)</sup>=IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3B((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4

Synonyms:IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4

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Chemical Property of IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4
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Technology Process of IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4

There total 2 articles about IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3<sup>(1+)</sup>*CF<sub>3</sub>SO<sub>3</sub><sup>(1-)</sup>=IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3CF<sub>3</sub>SO<sub>3</sub>
190650-43-2

IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*CF3SO3(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3CF3SO3

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
79060-88-1

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3<sup>(1+)</sup>*B((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4<sup>(1-)</sup>=IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3B((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4
190650-44-3

IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4

Guidance literature:
In dichloromethane; byproducts: NaOTf; Ir-complex was dissolved in CH2Cl2, ligand was added, mixt. was stirred overnight under N2; filtered, volatiles were removed in vacuo, recrystd. from CH2Cl2/toluene;
DOI:10.1021/om9910064

Reference yield: 63.0%

C<sub>5</sub>(CH<sub>3</sub>)5(P(CH<sub>3</sub>)3)Ir(CH<sub>3</sub>)(B(C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2)4)

C5(CH3)5(P(CH3)3)Ir(CH3)(B(C6H3(CF3)2)4)

1-Adamantanecarbaldehyde
2094-74-8

1-Adamantanecarbaldehyde

IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3<sup>(1+)</sup>*B((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4<sup>(1-)</sup>=IrC<sub>5</sub>(CH<sub>3</sub>)5P(CH<sub>3</sub>)3CO(CH<sub>2</sub>)6C(CH)3B((CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4
190650-44-3

IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*B((CF3)2C6H3)4(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3B((CF3)2C6H3)4

Guidance literature:
With methane; In dichloromethane; reaction at 25°C for minutes; recrystn. (2x);
DOI:10.1021/ja970245k
upstream raw materials:

1-Adamantanecarbaldehyde

IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3(1+)*CF3SO3(1-)=IrC5(CH3)5P(CH3)3CO(CH2)6C(CH)3CF3SO3

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

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