((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane

Base Information

• Chemical Name: ((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane
• CAS No.: 85613-11-2
• Molecular Formula: C₁₇H₂₆O₃Si
• Molecular Weight: 306.477

Synonyms:((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane

Chemical Property of ((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane

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Technology Process of ((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane

There total 1 articles about ((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

1-methoxy-2-methyl-3-trimethylsiloxy-1,3-pentadiene (72486-93-2) + benzaldehyde (100-52-7) → ((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane (85613-11-2)

Guidance literature:

tris(6,6,7,7,8,8-heptafluoro-2,2-dimethyl-3,5-octadionato)europium(III); In chloroform-d1; Ambient temperature;

DOI:10.1021/ja00349a064

Reference yield: 60.0%

((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane (85613-11-2) → (2S*,3S*)-2-phenyl-3,5-dimethyl-2,3-dihydro-4H-pyran-4-one (83378-98-7)

Guidance literature:

With trifluoroacetic acid; In diethyl ether;

DOI:10.1021/ja00349a064

Reference yield:

((2R,3R,6S)-6-Methoxy-3,5-dimethyl-2-phenyl-3,6-dihydro-2H-pyran-4-yloxy)-trimethyl-silane (85613-11-2) → (2R,3S,5S,6S)-2-Methoxy-3,5-dimethyl-6-phenyl-tetrahydro-pyran-4-one

Guidance literature:

With triethylamine; In methanol; Yield given;

DOI:10.1021/ja00349a064

upstream raw materials:

1-methoxy-2-methyl-3-trimethylsiloxy-1,3-pentadiene

benzaldehyde

Downstream raw materials:

(2S*,3S*)-2-phenyl-3,5-dimethyl-2,3-dihydro-4H-pyran-4-one

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