5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol

Base Information

Chemical Name:5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol
CAS No.:1042447-91-5
Molecular Formula:C₁₆H₁₇F₉O
Molecular Weight:396.296
Hs Code.:

Synonyms:5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol

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Chemical Property of 5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol

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Technology Process of 5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol

There total 2 articles about 5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1042447-78-8
1-cyclohexyl-2-iodo-4,4,5,5,6,6,7,7,7-nonafluoro-1-heptene

: 107-19-7
propargyl alcohol

: 1042447-91-5
5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol

: 1042448-04-3
5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(Z)-en-2-ynol

Guidance literature:: With copper(l) iodide; diethylamine; bis-triphenylphosphine-palladium(II) chloride; at 40 ℃; for 7h;
DOI:10.1016/j.tet.2008.04.057

Reference yield:

: 423-39-2
1-iodo-2,2,3,3,4,4,5,5,5-nonafluorobutane

: 5664-17-5
cyclohexylallene

: 107-19-7
propargyl alcohol

: 1042448-17-8
1-cyclohexyl-2-iodo-4,4,5,5,6,6,7,7,7-nonafluoro-1(Z)-heptene

: 1042447-91-5
5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(E)-en-2-ynol

: 1042448-04-3
5-cyclohexyl-4-(2',2',3',3',4',4',5',5',5'-nonafluoropentyl)pent-4(Z)-en-2-ynol

Guidance literature:: 1-iodo-2,2,3,3,4,4,5,5,5-nonafluorobutane; cyclohexylallene; With sodium dithionite; sodium hydrogencarbonate; In 1,4-dioxane; water; at 40 - 45 ℃; for 9h;

propargyl alcohol; With copper(l) iodide; diethylamine; bis-triphenylphosphine-palladium(II) chloride; In acetonitrile; at 0 ℃; for 1h; Further stages.;
DOI:10.1016/j.tet.2008.04.057