(R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid

Base Information

• Chemical Name: (R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid
• CAS No.: 858675-87-3
• Molecular Formula: C₁₈H₂₁N₃O₉S₃
• Molecular Weight: 519.577

Synonyms:(R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid

Chemical Property of (R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid

Chemical Property:

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Technology Process of (R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid

There total 2 articles about (R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C75H63N3O9S3 → (R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid (858675-87-3)

Guidance literature:

C₇₅H₆₃N₃O₉S₃; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

With triethylsilane; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1039/d1tc01445e

Reference yield: 58.0%

2-[3,5-bis-(1-tert-butoxycarbonyl-2-tritylsulfanyl-ethylcarbamoyl)-benzoylamino]-3-tritylsulfanyl-propionic acid tert-butyl ester → (R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid (858675-87-3)

Guidance literature:

With trifluoroacetic acid; ethanethiol; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/ol0507524

Reference yield:

(R)-2-[3,5-Bis-((R)-1-carboxy-2-mercapto-ethylcarbamoyl)-benzoylamino]-3-mercapto-propionic acid (858675-87-3) + N-acetylcystein (616-91-1,7696-05-1) + (2S,2'S)-N1,N1’-(1,3-phenylene)bis(2-(2-mercaptoacetamido)succinamide) (1597415-37-6) → N,N'-diacetyl-L-cystine (5545-17-5) + C28H38N8O12S4 + C33H42N6O18S6 + C41H48N10O18S6

Guidance literature:

In dimethyl sulfoxide; at 20 ℃; for 24h; pH=6.5;

DOI:10.1039/c4cc00245h

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