TH₀₄₀₉₂-014

Base Information

Chemical Name:TH₀₄₀₉₂-014
CAS No.:1431961-08-8
Molecular Formula:C₂₆H₃₃N₅O₂S
Molecular Weight:479.646
Hs Code.:

Synonyms:TH₀₄₀₉₂-014

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TH₀₄₀₉₂-014

Chemical Property:

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Technology Process of TH₀₄₀₉₂-014

There total 9 articles about TH₀₄₀₉₂-014 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1431959-92-0
C₉H₇N₃S

: 1431961-07-7
TH₀₄₀₉₂-008

: 1431961-08-8
TH₀₄₀₉₂-014

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 888498-07-5
(1H-pyrrolo[2,3-b]pyridin-4-yl)methanamine

: 1431961-08-8
TH₀₄₀₉₂-014

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; dmap / methanol / 0.5 h / 20 °C / Cooling with ice

1.2: 1.58 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 20 °C

With dmap; triethylamine; In methanol; dichloromethane;

Reference yield:

: 162356-90-3
N-(tert-butoxycarbonyl)-2-bromobenzylamine

: 1431961-08-8
TH₀₄₀₉₂-014

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,4-dioxane / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

3.1: Raney Ni / methanol / 16 h

3.2: 16 h / 827.46 Torr

4.1: trifluoroacetic acid / dichloromethane / 20 °C

4.2: 20 °C

5.1: triethylamine / dichloromethane / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; sodium carbonate; triethylamine; trifluoroacetic acid; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;