dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester

Base Information

• Chemical Name: dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester
• CAS No.: 245366-92-1
• Molecular Formula: C₁₉H₂₇N₃O₇S
• Molecular Weight: 441.505

Synonyms:dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester

Chemical Property of dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester

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Technology Process of dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester

There total 3 articles about dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(chloromethyl)-2-hydroxy-5-nitrobenzaldehyde (16644-30-7) → dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester (245366-92-1)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 15 h / 0 - 20 °C

2: triethylamine / dimethylformamide / 15 h / 0 - 20 °C

3: toluene / 6 h / Heating

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1: Alkylation / 2: Substitution / 3: Isomerization;

DOI:10.1021/jo000175r

Reference yield:

1,4,7-trioxa-10-azacyclododecane (41775-76-2) → dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester (245366-92-1)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 15 h / 0 - 20 °C

2: triethylamine / dimethylformamide / 15 h / 0 - 20 °C

3: toluene / 6 h / Heating

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1: Alkylation / 2: Substitution / 3: Isomerization;

DOI:10.1021/jo000175r

Reference yield:

dimethyl-thiocarbamic acid O-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester (245366-91-0) → dimethyl-thiocarbamic acid S-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester (245366-92-1)

Guidance literature:

In toluene; Heating;

DOI:10.1039/a903877i

upstream raw materials:

dimethyl-thiocarbamic acid O-[2-formyl-4-nitro-6-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-phenyl] ester

3-(chloromethyl)-2-hydroxy-5-nitrobenzaldehyde

1,4,7-trioxa-10-azacyclododecane

Downstream raw materials:

2-mercapto-5-nitro-3-(1,4,7-trioxa-10-aza-cyclododec-10-ylmethyl)-benzaldehyde

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