(S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide

Base Information

• Chemical Name: (S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide
• CAS No.: 459864-79-0
• Molecular Formula: C₃₆H₄₃NO₅
• Molecular Weight: 569.741

Synonyms:(S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide

Chemical Property of (S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of (S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide

There total 2 articles about (S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

4-hydroxy-4’-undecyloxybiphenyl (501414-42-2) + (S)-N-(1-methylpropyl)-5-carboxy-2,3-dihydro-1H-isoindole-1,3-dione (459864-85-8) → (S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide (459864-79-0)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1039/b111391g

Reference yield:

trimellitic Anhydride (552-30-7,145253-53-8) → (S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide (459864-79-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / DMA / 10 h / Heating

2: 86 percent / DCC / CH₂Cl₂

With 2,4-dichlorophenoxyacetic acid dimethylamine; dicyclohexyl-carbodiimide; In dichloromethane;

DOI:10.1039/b111391g

Reference yield: 22.0%

(S)-N-(1-methylpropyl)-4-[(4'-undecyloxybiphenyl-4-yl)oxycarbonyl]phthalimide (459864-79-0) → 2-sec-butyl-1-oxo-3-thioxo-2,3-dihydro-1H-isoindole-5-carboxylic acid 4'-undecyloxy-biphenyl-4-yl ester + 2-sec-butyl-3-oxo-1-thioxo-2,3-dihydro-1H-isoindole-5-carboxylic acid 4'-undecyloxy-biphenyl-4-yl ester + 2-sec-butyl-1,3-dithioxo-2,3-dihydro-1H-isoindole-5-carboxylic acid 4'-undecyloxy-biphenyl-4-yl ester

Guidance literature:

With Lawessons reagent;

DOI:10.1039/b111391g

upstream raw materials:

4-hydroxy-4’-undecyloxybiphenyl

(S)-N-(1-methylpropyl)-5-carboxy-2,3-dihydro-1H-isoindole-1,3-dione

trimellitic Anhydride

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