3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate

Base Information

Chemical Name:3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate
CAS No.:1430413-14-1
Molecular Formula:C₁₄H₂₆NO₅P
Molecular Weight:319.338
Hs Code.:

Synonyms:3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate

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Chemical Property of 3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate

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Technology Process of 3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate

There total 5 articles about 3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1430413-53-8
1-(3-hydroxypropoxy)cyclohexanecarbonitrile

: 814-49-3
diethyl chlorophosphate

: 1430413-14-1
3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate

Guidance literature:: With 1-methyl-1H-imidazole; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol400788q

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 1430413-14-1
3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide / tetrahydrofuran / -40 - 0 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere

3: 1-methyl-1H-imidazole / tetrahydrofuran / 0 °C / Inert atmosphere

With 1-methyl-1H-imidazole; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tetrabutyl ammonium fluoride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ol400788q

Reference yield:

: 1430413-00-5
1-(3-((tert-butyldimethylsilyl)oxy)propoxy)cyclohexanecarbonitrile

: 1430413-14-1
3-((1-cyanocyclohexyl)oxy)propyl diethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere

2: 1-methyl-1H-imidazole / tetrahydrofuran / 0 °C / Inert atmosphere

With 1-methyl-1H-imidazole; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/ol400788q