C₂₉H₃₂N₂O₁₁Si

Base Information

• Chemical Name: C₂₉H₃₂N₂O₁₁Si
• CAS No.: 1574349-94-2
• Molecular Formula: C₂₉H₃₂N₂O₁₁Si
• Molecular Weight: 612.665
• Mol file: 1574349-94-2.mol

Synonyms:C₂₉H₃₂N₂O₁₁Si

Chemical Property of C₂₉H₃₂N₂O₁₁Si

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₉H₃₂N₂O₁₁Si

There total 3 articles about C₂₉H₃₂N₂O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

C15H26O3Si (1574349-93-1) + 4-Nitrophenyl chloroformate (7693-46-1) → C29H32N2O11Si (1574349-94-2)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ol5003412

Reference yield:

2,6-bis(hydroxymethyl)-4-methylphenol (91-04-3) → C29H32N2O11Si (1574349-94-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

2: toluene-4-sulfonic acid / methanol / 20 °C

3: triethylamine; dmap / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; dmap; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1021/ol5003412

Reference yield:

C27H54O3Si3 (1574349-92-0) → C29H32N2O11Si (1574349-94-2)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / methanol / 20 °C

2: triethylamine; dmap / tetrahydrofuran / 0 - 20 °C

With dmap; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol;

DOI:10.1021/ol5003412

upstream raw materials:

2,6-bis(hydroxymethyl)-4-methylphenol

C₁₅H₂₆O₃Si

4-Nitrophenyl chloroformate

C₂₇H₅₄O₃Si₃