N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

Base Information

Chemical Name:N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide
CAS No.:1408236-54-3
Molecular Formula:C₄₈H₅₂N₂O₉S₂
Molecular Weight:865.081
Hs Code.:

Synonyms:N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

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Technology Process of N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

There total 1 articles about N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 103213-32-7,167015-11-4
N-(9-fluorenylmethoxycarbonyl)-S-trityl-L-cysteine

: 182358-65-2
3-(2-aminoethylthio)propyl α-D-mannopyranoside

: 1408236-54-3
N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2ob26118a

Reference yield: 67.0%

: 1408236-54-3
N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

: 1408236-55-4
S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

Guidance literature:: With morpholine; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2ob26118a

Reference yield:

: 1408236-54-3
N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

: 1408236-56-5
N-(acetyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

Guidance literature:: Multi-step reaction with 2 steps

1: morpholine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

2: pyridine / 20 °C

With morpholine; pyridine; In N,N-dimethyl-formamide;
DOI:10.1039/c2ob26118a