S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

Base Information

• Chemical Name: S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide
• CAS No.: 1408236-55-4
• Molecular Formula: C₃₃H₄₂N₂O₇S₂
• Molecular Weight: 642.838

Synonyms:S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

Chemical Property of S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

Chemical Property:

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Technology Process of S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

There total 3 articles about S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide (1408236-54-3) → S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide (1408236-55-4)

Guidance literature:

With morpholine; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1039/c2ob26118a

Reference yield:

N-(9-fluorenylmethoxycarbonyl)-S-trityl-L-cysteine (103213-32-7,167015-11-4) → S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide (1408236-55-4)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: morpholine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With morpholine; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide;

DOI:10.1039/c2ob26118a

Reference yield:

3-(2-aminoethylthio)propyl α-D-mannopyranoside (182358-65-2) → S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide (1408236-55-4)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: morpholine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With morpholine; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide;

DOI:10.1039/c2ob26118a

upstream raw materials:

N-(9H-fluoren-9-ylmethoxycarbonyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

N-(9-fluorenylmethoxycarbonyl)-S-trityl-L-cysteine

3-(2-aminoethylthio)propyl α-D-mannopyranoside

Downstream raw materials:

N-(acetyl)-S-(triphenylmethyl)-L-cysteine-[6-(α-D-mannopyranosyloxy)-3-thiahexyl]amide

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