C₂H₁₁B₁₀(C₆H₉)

Base Information

Chemical Name:C₂H₁₁B₁₀(C₆H₉)
CAS No.:127085-62-5
Molecular Formula:C₈H₂₀B₁₀
Molecular Weight:224.357
Hs Code.:

C<sub>2</sub>H<sub>11</sub>B<sub>10</sub>(C<sub>6</sub>H<sub>9</sub>)

Synonyms:C₂H₁₁B₁₀(C₆H₉)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂H₁₁B₁₀(C₆H₉)

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Technology Process of C₂H₁₁B₁₀(C₆H₉)

There total 3 articles about C₂H₁₁B₁₀(C₆H₉) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: C₉H₁₈B₁₀O₃S

: 110-83-8
cyclohexene

: 127085-62-5
C₂H₁₁B₁₀(C₆H₉)

Guidance literature:: With lithium hexamethyldisilazane; In cyclohexane; at 20 ℃; for 0.0333333h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.1c00649

Reference yield: 67.0%

: 14264-16-5,53996-95-5,62075-39-2,39716-73-9
bis(triphenylphosphine)nickel(II) chloride

: 109-72-8,29786-93-4
n-butyllithium

: 16872-09-6
1,2-dicarba-closo-dodecaborane⁽¹²⁾

: 110-83-8
cyclohexene

: 127085-62-5
C₂H₁₁B₁₀(C₆H₉)

Guidance literature:: In tetrahydrofuran; Ni complex was added to soln. Li2C2B10H10 in THF (from C2B10H12 and n-BuLi), mixt. was stirred at room temp. for 0.5 h, alkene was added, mixt. was heated at 90°C overnight; ppt. was removed, soln. was evapd. in vac., residue was chromd. on silica;
DOI:10.1002/anie.200801958