benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate

Base Information

Chemical Name:benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate
CAS No.:1647153-59-0
Molecular Formula:C₂₄H₂₉NO₅
Molecular Weight:411.498
Hs Code.:

Synonyms:benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate

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Chemical Property of benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate

Chemical Property:

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Technology Process of benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate

There total 6 articles about benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1647153-57-8
(4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylic acid

: 100-39-0
benzyl bromide

: 1647153-59-0
benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.3762/bjoc.10.113

Reference yield:

: 1647153-56-7
(4R,5S)-N-(benzyloxycarbonyl)-4-(hydroxymethyl)-5-isopropyl-2,2-dimethyloxazolidine

: 1647153-59-0
benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ruthenium trichloride; sodium periodate / water; tetrachloromethane; acetonitrile / 5 h / 0 °C

2: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With ruthenium trichloride; sodium periodate; caesium carbonate; In tetrachloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3762/bjoc.10.113

Reference yield:

: 1647153-55-6
(4R,5S)-N-(benzyloxycarbonyl)-4-(tert-butyldimethylsilyloxymethyl)-5-isopropyl-2,2-dimethyloxazolidine

: 1647153-59-0
benzyl (4S,5S)-N-(benzyloxycarbonyl)-5-isopropyl-2,2-dimethyloxazolidine-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 19 h / 20 °C

2: ruthenium trichloride; sodium periodate / water; tetrachloromethane; acetonitrile / 5 h / 0 °C

3: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With ruthenium trichloride; sodium periodate; tetrabutyl ammonium fluoride; caesium carbonate; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3762/bjoc.10.113