C₁₅H₁₁FN₂O₃S

Base Information

Chemical Name:C₁₅H₁₁FN₂O₃S
CAS No.:1278405-50-7
Molecular Formula:C₁₅H₁₁FN₂O₃S
Molecular Weight:318.328
Hs Code.:

C<sub>15</sub>H<sub>11</sub>FN<sub>2</sub>O<sub>3</sub>S

Synonyms:C₁₅H₁₁FN₂O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₁FN₂O₃S

Chemical Property:

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Technology Process of C₁₅H₁₁FN₂O₃S

There total 4 articles about C₁₅H₁₁FN₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1278405-49-4
C₁₇H₁₅FO₅S

: 1278405-50-7
C₁₅H₁₁FN₂O₃S

Guidance literature:: With hydrazine; In ethanol; at 20 - 60 ℃;

Reference yield:

: 88-13-1
3-Thiophene carboxylic acid

: 1278405-50-7
C₁₅H₁₁FN₂O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid; pyridinium hydrobromide perbromide; hydrogen bromide / 24 h / 20 °C

2: sulfuric acid / 24 h / Reflux

3: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / Reflux; Inert atmosphere

4: lithium diisopropyl amide / tetrahydrofuran / 1 h / -50 - -40 °C / Inert atmosphere

5: hydrazine hydrate / ethanol / 24 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; pyridinium hydrobromide perbromide; sulfuric acid; hydrogen bromide; sodium carbonate; hydrazine hydrate; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1016/j.bioorg.2022.105704

Reference yield:

: 100523-84-0
2-bromothiophene-4-carboxylic acid

: 1278405-50-7
C₁₅H₁₁FN₂O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 24 h / Reflux

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / Reflux; Inert atmosphere

3: lithium diisopropyl amide / tetrahydrofuran / 1 h / -50 - -40 °C / Inert atmosphere

4: hydrazine hydrate / ethanol / 24 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; sodium carbonate; hydrazine hydrate; lithium diisopropyl amide; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1016/j.bioorg.2022.105704