Technology Process of C19H21N3O4S
There total 12 articles about C19H21N3O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydroxide / acetone; water / 0 °C / pH 10.8 - 11
1.2: 2 h / 0 °C
2.1: trifluoro-[1,3,5]triazine; pyridine / dichloromethane / 2 h / -10 °C
3.1: quinoline / dichloromethane / 48 h / 55 °C
4.1: hydrogen; 5%-palladium/activated carbon / ethanol / 2.5 h / 760.05 Torr
5.1: acetic acid / 200 °C / Microwave irradiation
6.1: chloroform / 20 h / 65 °C
7.1: pyridine / 16 h / 70 °C
With
pyridine; quinoline; trifluoro-[1,3,5]triazine; 5%-palladium/activated carbon; hydrogen; acetic acid; sodium hydroxide;
In
ethanol; dichloromethane; chloroform; water; acetone;
DOI:10.1016/j.bmcl.2013.02.084
- Guidance literature:
-
Multi-step reaction with 2 steps
1: chloroform / 20 h / 65 °C
2: pyridine / 16 h / 70 °C
With
pyridine;
In
chloroform;
DOI:10.1016/j.bmcl.2013.02.084
- Guidance literature:
-
Multi-step reaction with 6 steps
1: trifluoro-[1,3,5]triazine; pyridine / dichloromethane / 2 h / -10 °C
2: quinoline / dichloromethane / 48 h / 55 °C
3: hydrogen; 5%-palladium/activated carbon / ethanol / 2.5 h / 760.05 Torr
4: acetic acid / 200 °C / Microwave irradiation
5: chloroform / 20 h / 65 °C
6: pyridine / 16 h / 70 °C
With
pyridine; quinoline; trifluoro-[1,3,5]triazine; 5%-palladium/activated carbon; hydrogen; acetic acid;
In
ethanol; dichloromethane; chloroform;
DOI:10.1016/j.bmcl.2013.02.084
