phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

Base Information

Chemical Name:phosphorodichloridic acid, 2-bromo-2-phenylethyl ester
CAS No.:99884-77-2
Molecular Formula:C₈H₈BrCl₂O₂P
Molecular Weight:317.934
Hs Code.:

Synonyms:phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

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Chemical Property of phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

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Technology Process of phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

There total 1 articles about phosphorodichloridic acid, 2-bromo-2-phenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41252-83-9
2-bromo-2-phenylethanol

: 99884-77-2
phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

Guidance literature:: With trichlorophosphate; In tetrachloromethane; at 30 ℃; for 76h;
DOI:10.1021/jm00153a005

Reference yield:

: 87233-21-4,99945-82-1
<2-Hexadecyloxy-1-(hydroxymethyl)ethyl> acetate

: 99884-77-2
phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

: Acetic acid 2-[(2-bromo-2-phenyl-ethoxy)-chloro-phosphoryloxy]-1-hexadecyloxymethyl-ethyl ester

Guidance literature:: With triethylamine; In tetrachloromethane; at 0 ℃; for 18h;
DOI:10.1021/jm00153a005

Reference yield:

: 99884-77-2
phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

: C₃₂H₅₈NO₇P

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CCl₄ / 18 h / 0 °C

2: 0.5 M NaOAc / tetrahydrofuran / 2 h

3: dimethylformamide; acetonitrile / 18 h / 65 °C

With sodium acetate; triethylamine; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00153a005