2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester

Base Information

Chemical Name:2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester
CAS No.:118469-70-8
Molecular Formula:C₂₉H₅₀BrO₇P
Molecular Weight:621.59
Hs Code.:

Synonyms:2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester

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Chemical Property of 2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester

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Technology Process of 2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester

There total 3 articles about 2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid 2-[(2-bromo-2-phenyl-ethoxy)-chloro-phosphoryloxy]-1-hexadecyloxymethyl-ethyl ester

: 118469-70-8
2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester

Guidance literature:: With sodium acetate; In tetrahydrofuran; for 2h;
DOI:10.1021/jm00153a005

Reference yield:

: 41252-83-9
2-bromo-2-phenylethanol

: 118469-70-8
2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃ / CCl₄ / 76 h / 30 °C

2: Et₃N / CCl₄ / 18 h / 0 °C

3: 0.5 M NaOAc / tetrahydrofuran / 2 h

With sodium acetate; triethylamine; trichlorophosphate; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jm00153a005

Reference yield:

: 99884-77-2
phosphorodichloridic acid, 2-bromo-2-phenylethyl ester

: 118469-70-8
2-(acetyloxy)-3-(hexadecyloxy)propyl-phosphoric acid, 2-bromo-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CCl₄ / 18 h / 0 °C

2: 0.5 M NaOAc / tetrahydrofuran / 2 h

With sodium acetate; triethylamine; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jm00153a005