Technology Process of 5,15-bis-(4-methylphenyl)-10,20-diphenyl-porphyrin
There total 36 articles about 5,15-bis-(4-methylphenyl)-10,20-diphenyl-porphyrin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
at 85 ℃;
for 7h;
DOI:10.1039/b201622b
- Guidance literature:
-
5-phenyldipyrromethane; 1,9-bis[α-hydroxy-α-(p-tolyl)methyl]-5-phenyldipyrromethane;
With
ytterbium(III) triflate;
In
dichloromethane;
at 20 ℃;
for 0.5h;
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
at 20 ℃;
for 1h;
DOI:10.1021/jo035622s
- Guidance literature:
-
10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane;
With
sodium tetrahydroborate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 0.666667h;
With
ytterbium(III) triflate;
In
dichloromethane;
at 20 ℃;
for 0.5 - 1h;
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
at 20 ℃;
for 1h;
Product distribution / selectivity;
