10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane

Base Information

• Chemical Name: 10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane
• CAS No.: 750646-90-3
• Molecular Formula: C₃₁H₃₇BN₂O
• Molecular Weight: 464.459
• Mol file: 750646-90-3.mol

Synonyms:10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane

Chemical Property of 10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane

Chemical Property:

Purity/Quality:

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Technology Process of 10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane

There total 1 articles about 10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

di-n-butylboryl trifluoromethanesulfonate (60669-69-4) + 1-(p-methylbenzoyl)-5-phenyldipyrromethane (171523-03-8) → 10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane (750646-90-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.5 - 1h;

Reference yield: 26.0%

10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane (750646-90-3) → 5,15-bis-(4-methylphenyl)-10,20-diphenyl-porphyrin (132313-39-4)

Guidance literature:

10-(dibutylboryl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane; With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 0.666667h;

With ytterbium(III) triflate; In dichloromethane; at 20 ℃; for 0.5 - 1h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h; Product distribution / selectivity;

upstream raw materials:

di-n-butylboryl trifluoromethanesulfonate

1-(p-methylbenzoyl)-5-phenyldipyrromethane

Downstream raw materials:

5,15-bis-(4-methylphenyl)-10,20-diphenyl-porphyrin