N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide

Base Information

Chemical Name:N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide
CAS No.:1271801-20-7
Molecular Formula:C₂₃H₂₃N₅O₂S
Molecular Weight:433.534
Hs Code.:

Synonyms:N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide

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Chemical Property of N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide

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Technology Process of N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide

There total 4 articles about N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1271808-60-6
C₃₀H₂₉N₅O₄S₂

: 1271801-20-7
N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide

Guidance literature:: With methanol; water; potassium carbonate; at 65 ℃; for 6h;

Reference yield:

: 1271808-46-8
C₃₂H₃₁N₅O₄S

: 1271801-20-7
N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C

2: triethylamine / tetrahydrofuran / 12 h / 20 °C

3: potassium carbonate; water; methanol / 6 h / 65 °C

With methanol; water; hydrogen; potassium carbonate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol;

Reference yield:

: 908334-19-0
3-(1-tert-butoxycarbonyl-3-piperidyl)benzoic acid

: 1271801-20-7
N-(3-(1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-3-yl)phenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; diphenyl phosphoryl azide / toluene / 80 °C

2.1: hydrogenchloride / 1,4-dioxane / 20 °C

2.2: 4 h / 90 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C

4.1: triethylamine / tetrahydrofuran / 12 h / 20 °C

5.1: potassium carbonate; water; methanol / 6 h / 65 °C

With hydrogenchloride; methanol; diphenyl phosphoryl azide; water; hydrogen; potassium carbonate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; toluene;