C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)

Base Information

Chemical Name:C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)
CAS No.:912290-06-3
Molecular Formula:C₁₆H₁₆N₂O₂
Molecular Weight:268.315
Hs Code.:

C<sub>5</sub>H<sub>4</sub>NCHNCH(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)(COOCH<sub>3</sub>)

Synonyms:C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)

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Chemical Property of C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)

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Technology Process of C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)

There total 1 articles about C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143745-68-0
2-methyl-1-(2-methylphenyl)-2-propanamine

: 15028-44-1
DL-phenylalanine methyl ester

: 912290-06-3
C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)

Guidance literature:: In toluene; at 80 ℃; for 4h; Molecular sieve; Sealed tube;
DOI:10.1039/c9ra05670j

Reference yield: 87.0%

: 941-69-5
N-phenyl-maleimide

: 912290-06-3
C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)

: methyl 1-benzyl-4,6-dioxo-5-phenyl-3-(pyridin-2-yl)octahydropyrrolo[3,4-c]pyrrole-1-carboxylate

Guidance literature:: With silver(I) acetate; In toluene; at 20 - 30 ℃; for 18h;
DOI:10.1055/s-0037-1611356

Reference yield:

: ammonium hexafluorophosphate

: 12128-23-3
tricarbonylcyclopentadienylmolybdenum(II) chloride

: 912290-06-3
C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)

: 72347-28-5
Mo(C₅H₅)(CO)2C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)⁽¹⁺⁾*PF₆^(1-)=Mo(C₅H₅)(CO)2C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)PF₆

: 72377-53-8
Mo(C₅H₅)(CO)2C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)⁽¹⁺⁾*PF₆^(1-)=Mo(C₅H₅)(CO)2C₅H₄NCHNCH(CH₂C₆H₅)(COOCH₃)PF₆

Guidance literature:: In ethanol; water; benzene; byproducts: CO; soln. of C5H5Mo(CO)3Cl and Schiff base in benzene refluxed until theor.quantity of CO liberated, crystals of chloride sepd. out, they filteredoff, dissolved in min. amt. of EtOH, after filtration water then NH4PF6added to stirred soln.; mixt. of RS'/SR'/SS'/RR' isomers heated in a min. amt. of mixt. of acetone-CH2Cl2-ether needed to dissolution, cooling the system to -25°C for 15 h, obtained solid fraction enriched in the less sol. RS'/SR' isomers, sepn. can be monitored by NMR;