(S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester

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Chemical Name:(S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester
CAS No.:914605-75-7
Molecular Formula:C₃₄H₅₅N₃O₆
Molecular Weight:601.827
Hs Code.:

Synonyms:(S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester

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Chemical Property of (S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester

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Technology Process of (S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester

There total 9 articles about (S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914604-30-1
(S)-amino-cyclohexyl-acetic acid cyclopentyl ester

: 914605-64-4
octanedioic acid (4-formyl-phenyl)-amide (1-isobutoxy-ethoxy)-amide

: 914605-75-7
(S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester

Guidance literature:: (S)-amino-cyclohexyl-acetic acid cyclopentyl ester; octanedioic acid (4-formyl-phenyl)-amide (1-isobutoxy-ethoxy)-amide; In methanol; at 20 ℃;

With sodium tetrahydroborate; In methanol; for 0.25h;

With sodium hydroxide; In methanol; water;

Reference yield:

: 914605-63-3
octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

: 914605-75-7
(S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: manganese(IV) oxide / dichloromethane / 1.5 h / 20 °C

2.1: methanol / 20 °C

2.2: 0.25 h

With manganese(IV) oxide; In methanol; dichloromethane;

Reference yield:

: 860216-27-9
O-(1-isobutoxyethyl)hydroxylamine

: 914605-75-7
(S)-cyclohexyl-{4-[7-(1-isobutoxy-ethoxycarbamoyl)-heptanoylamino]-benzylamino}-acetic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran; dichloromethane / 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran / 3 h / 50 °C

3.1: N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C

4.1: manganese(IV) oxide / dichloromethane / 1.5 h / 20 °C

5.1: methanol / 20 °C

5.2: 0.25 h

With manganese(IV) oxide; lithium hydroxide; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;