octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

Base Information

Chemical Name:octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide
CAS No.:914605-63-3
Molecular Formula:C₂₁H₃₄N₂O₅
Molecular Weight:394.511
Hs Code.:

Synonyms:octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

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Chemical Property of octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

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Technology Process of octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

There total 5 articles about octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 914605-62-2
7-(1-isobutoxy-ethoxycarbamoyl)-heptanoic acid

: 403613-26-3
4-trimethylsilanyloxymethyl-phenylamine

: 914605-63-3
octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 860216-27-9
O-(1-isobutoxyethyl)hydroxylamine

: 914605-63-3
octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran; dichloromethane / 20 °C

2: lithium hydroxide; water / tetrahydrofuran / 3 h / 50 °C

3: N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C

With lithium hydroxide; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 623-04-1
4-aminobenzenemethanol

: 914605-63-3
octanedioic acid (4-hydroxymethyl-phenyl)-amide (1-isobutoxyethoxy)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 20 °C

2: N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide;