3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine

Base Information

Chemical Name:3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine
CAS No.:302788-34-7
Molecular Formula:C₃₀H₃₃NO₅
Molecular Weight:487.596
Hs Code.:

Synonyms:3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine

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Chemical Property of 3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine

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Technology Process of 3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine

There total 7 articles about 3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-46-9
benzylamine

: 302788-33-6
3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydo-hexos-5-ulo-2,5-furanose

: 302788-34-7
3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine

Guidance literature:: With 4 A molecular sieve; In dichloromethane; at 4 ℃; for 3h;
DOI:10.1021/jo0203903

Reference yield:

: 302788-32-5
1,4-di-O-benzyl-2,3-O-isopropylidene-α-L-sorbofuranose

: 302788-34-7
3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

2: 100 percent / molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 4 °C

With 4 A molecular sieve; Dess-Martin periodane; In dichloromethane;
DOI:10.1021/jo0203903

Reference yield:

: 473931-75-8
1,4-di-O-benzyl-2,3-O-isopropylidene-6-O-triphenylmethyl-α-L-sorbofuranose

: 302788-34-7
3,6-di-O-benzyl-4,5-O-isopropylidene-D-xylo-aldehydohexos-5-ulo-2,5-furanose N-benzylimine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / HBr / acetic acid / 10 - 15 °C

2: 91 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 20 °C

3: 100 percent / molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 4 °C

With 4 A molecular sieve; hydrogen bromide; Dess-Martin periodane; In dichloromethane; acetic acid;
DOI:10.1021/jo0203903