3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Base Information

Chemical Name:3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate
CAS No.:1373433-81-8
Molecular Formula:C₇H₇O₃S*C₂₂H₃₉N₂O₅
Molecular Weight:582.759
Hs Code.:

Synonyms:3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

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Chemical Property of 3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Chemical Property:

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Technology Process of 3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

There total 6 articles about 3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1226913-37-6
benzyl 4-(dimethylamino)-2-methylbutan-2-ylcarbamate

: 62921-74-8,518012-62-9,58320-73-3
2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate

: 1373433-81-8
3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Guidance literature:: at 45 ℃;

Reference yield:

: 105090-72-0
3-azido-3-methylbutanoic acid

: 1373433-81-8
3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 1,2-dichloro-ethane / 2 h / 50 °C

2.1: dichloromethane; water / 1 h / 0 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 22 h / 20 - 70 °C / Cooling with ice

3.2: 0.33 h / Cooling with ice

3.3: 0.33 h

4.1: tetrahydrofuran / 17 h / 20 °C

5.1: 45 °C

With lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 1373433-81-8
3-(((benzyloxy)carbonyl)amino)-N-(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-N,N,3-trimethylbutan-1-aminium 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide / water / 49 h / 20 - 95 °C

2.1: thionyl chloride / 1,2-dichloro-ethane / 2 h / 50 °C

3.1: dichloromethane; water / 1 h / 0 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 22 h / 20 - 70 °C / Cooling with ice

4.2: 0.33 h / Cooling with ice

4.3: 0.33 h

5.1: tetrahydrofuran / 17 h / 20 °C

6.1: 45 °C

With lithium aluminium tetrahydride; thionyl chloride; sodium azide; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;