N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

Base Information

• Chemical Name: N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine
• CAS No.: 1609962-95-9
• Molecular Formula: C₁₅H₂₀N₄OS
• Molecular Weight: 304.416

Synonyms:N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

Chemical Property of N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

Chemical Property:

Purity/Quality:

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Technology Process of N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

There total 1 articles about N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-91-5) + cyclopropylboronic acid (411235-57-9) → N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-95-9)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; at 80 ℃;

Reference yield:

(S)-4-fluoro-2-(tetrahydrofuran-3-yloxy)aniline (1332712-64-7) + N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-95-9) → C23H25FN4O3S (1609960-59-9)

Guidance literature:

In acetic acid; at 75 ℃;

Reference yield:

N'-[2-cyano-3-cyclopropyl-5-[[dimethyl(oxo)-λ6-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine (1609962-95-9) + (3S,4S)-4-(2-amino-5-fluoro-phenoxy)-tetrahydro-furan-3-ol → C23H25FN4O4S

Guidance literature:

With acetic acid; at 80 ℃; for 5h;

upstream raw materials:

N'-[3-bromo-2-cyano-5-[[dimethyl(oxo)-λ⁶-sulfanylidene]amino]phenyl]-N,N-dimethyl-formamidine

cyclopropylboronic acid

Downstream raw materials:

C₂₃H₂₅FN₄O₃S

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