(2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

Base Information

Chemical Name:(2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate
CAS No.:360042-97-3
Molecular Formula:C₂₁H₃₃O₅P
Molecular Weight:398.448
Hs Code.:

(2Z,6E)-(1,1-2H<sub>2</sub>)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

Synonyms:(2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

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Chemical Property of (2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

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Technology Process of (2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

There total 3 articles about (2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 814-49-3
diethyl chlorophosphate

: 200397-73-5
(2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-ol

: 360042-97-3
(2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1016/S0040-4020(01)00451-3

Reference yield:

: 32989-52-9
(E)-4-methyl-6-(phenylmethoxy)-4-hexenal

: 360042-97-3
(2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 18-crown-6; KN[Si(CH₃)3]2 / tetrahydrofuran / 0.33 h / -78 °C

1.2: 93 percent / tetrahydrofuran / 0.5 h / -78 °C

2.1: 90 percent / LiAlD₄; AlCl₃ / diethyl ether / 0.5 h / -10 °C

3.1: 91 percent / pyridine / CH₂Cl₂ / 4 h / 0 °C

With pyridine; aluminium trichloride; lithium aluminium deuteride; 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)00451-3

Reference yield:

: 360043-10-3
ethyl (2E,6E)-8-benzyloxy-2,6-dimethyl-2,6-octadienoate

: 360042-97-3
(2Z,6E)-(1,1-2H₂)-8-benzyloxy-2,6-dimethyl-2,6-octadien-1-yl diethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / LiAlD₄; AlCl₃ / diethyl ether / 0.5 h / -10 °C

2: 91 percent / pyridine / CH₂Cl₂ / 4 h / 0 °C

With pyridine; aluminium trichloride; lithium aluminium deuteride; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)00451-3