(E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one

Base Information

Chemical Name:(E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one
CAS No.:1607855-08-2
Molecular Formula:C₁₈H₂₄N₂O
Molecular Weight:284.401
Hs Code.:

Synonyms:(E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one

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Chemical Property of (E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one

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Technology Process of (E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one

There total 1 articles about (E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 917-92-0
3,3-Dimethylbut-1-yne

: 1394172-80-5
C₁₂H₁₄N₂O

: 1607855-08-2
(E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one

Guidance literature:: With tris(triphenylphosphine)rhodium(I) chloride; In 1,4-dioxane; at 130 ℃; for 20h; stereoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c3cc47556e

Reference yield:

: 1607855-08-2
(E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one

: C₂₄H₃₅N₂O₃⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / Inert atmosphere

2: dichloromethane / -20 - 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3cc47556e

Reference yield:

: 1607855-08-2
(E)-3-(3,3-dimethylbut-1-en-1-yl)-6-methyl-2-(pyridin-2-ylamino)cyclohex-2-en-1-one

: 1607855-23-1
tert-butyl (E)-(2-(3,3-dimethylbut-1-en-1-yl)-5-methyl-6-oxocyclohex-1-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / Inert atmosphere

2: dichloromethane / -20 - 20 °C / Inert atmosphere

3: sodium hydroxide / methanol / 1 h / 50 °C

With sodium hydride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c3cc47556e