2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine

Base Information

Chemical Name:2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine
CAS No.:154878-68-9
Molecular Formula:C₃₆H₃₂N₂O₄Se
Molecular Weight:635.621
Hs Code.:

Synonyms:2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine

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Technology Process of 2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine

There total 2 articles about 2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142573-74-8
2'-deoxy-2'-methylidene-5'-O-trityl-5-methyluridine

: 154878-68-9
2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 0.33 h / 0 °C

2: ethanol / 0.5 h / Ambient temperature

With triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4020(01)80786-9

Reference yield:

: 23974-72-3
sodium phenylselenide

: Methanesulfonic acid (2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-methylene-2-trityloxymethyl-tetrahydro-furan-3-yl ester

: 154878-68-9
2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine

Guidance literature:: In ethanol; for 0.5h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4020(01)80786-9

Reference yield: 34.0%

: 4248-19-5
tert-butyl carbazate

: 154878-68-9
2',3'-didehydro-2',3'-dideoxy-2'-phenylselenomethyl-5'-O-trityl-5-methyluridine

: 142573-74-8
2'-deoxy-2'-methylidene-5'-O-trityl-5-methyluridine

: (3'S)-3'-tert-butoxycarbonylamino-2',3'-dideoxy-2'-methylidene-5'-O-trityl-5-methyluridine

Guidance literature:: With N-chloro-succinimide; triethylamine; In tetrahydrofuran; methanol; at -78 - -21 ℃; for 4h;
DOI:10.1016/S0040-4020(01)80786-9